Determination of trace elements in a human serum reference material by inductively coupled plasma mass spectrometry
Identifieur interne : 000448 ( Main/Exploration ); précédent : 000447; suivant : 000449Determination of trace elements in a human serum reference material by inductively coupled plasma mass spectrometry
Auteurs : RBID : ISTEX:604_1990_Article_BF01244693.pdfEnglish descriptors
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Abstract
A method was developed for the determination of Fe, Co, Cu, Zn, Rb, Mo and Cs in human serum by ICP-MS. Sample preparation was kept as limited as possible: Serum samples were diluted with nitric acid and indium was added as internal standard. The results for Fe, Co, Cu, and Zn were corrected for interferences from polyatomic ions using a suitable blank solution. No interferences occur for the considered isotopes of Rb, Mo, and Cs. A “second-generation human serum reference material” was analyzed, in order to test the accuracy and precision of the analytical procedure. The results obtained are in good agreement with the certified values.
DOI: 10.1007/BF01244693
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<record><TEI><teiHeader><fileDesc><titleStmt><title>Determination of trace elements in a human serum reference material by inductively coupled plasma mass spectrometry</title><author wicri:is="90%"><name>Hans Vanhoe</name><affiliation wicri:level="1"><mods:affiliation>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent, Belgium</mods:affiliation><country xml:lang="fr">Belgique</country><wicri:regionArea>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent</wicri:regionArea><wicri:noRegion>Gent</wicri:noRegion></affiliation></author><author wicri:is="80%"><name>Carlo Vandecasteele</name><affiliation wicri:level="1"><mods:affiliation>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent, Belgium</mods:affiliation><country xml:lang="fr">Belgique</country><wicri:regionArea>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent</wicri:regionArea><wicri:noRegion>Gent</wicri:noRegion></affiliation></author><author wicri:is="90%"><name>Jacques Versieck</name><affiliation wicri:level="1"><mods:affiliation>Department of Internal Medicine, Division of Gastroenterology, University Hospital, De Pintelaan 185, B-9000, Gent, Belgium</mods:affiliation><country xml:lang="fr">Belgique</country><wicri:regionArea>Department of Internal Medicine, Division of Gastroenterology, University Hospital, De Pintelaan 185, B-9000, Gent</wicri:regionArea><wicri:noRegion>Gent</wicri:noRegion></affiliation></author><author wicri:is="90%"><name>Richard Dams</name><affiliation wicri:level="1"><mods:affiliation>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent, Belgium</mods:affiliation><country xml:lang="fr">Belgique</country><wicri:regionArea>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent</wicri:regionArea><wicri:noRegion>Gent</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="RBID">ISTEX:604_1990_Article_BF01244693.pdf</idno><date when="1990">1990</date><idno type="doi">10.1007/BF01244693</idno><idno type="wicri:Area/Main/Corpus">000D56</idno><idno type="wicri:Area/Main/Curation">000D56</idno><idno type="wicri:Area/Main/Exploration">000448</idno></publicationStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Accuracy</term><term>Human serum</term><term>ICP-MS</term><term>Interferences</term><term>Trace elements</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="eng">A method was developed for the determination of Fe, Co, Cu, Zn, Rb, Mo and Cs in human serum by ICP-MS. Sample preparation was kept as limited as possible: Serum samples were diluted with nitric acid and indium was added as internal standard. The results for Fe, Co, Cu, and Zn were corrected for interferences from polyatomic ions using a suitable blank solution. No interferences occur for the considered isotopes of Rb, Mo, and Cs. A “second-generation human serum reference material” was analyzed, in order to test the accuracy and precision of the analytical procedure. The results obtained are in good agreement with the certified values.</div></front></TEI><mods xsi:schemaLocation="http://www.loc.gov/mods/v3 file:///applis/istex/home/loadistex/home/etc/xsd/mods.xsd" version="3.4" istexId="ea3bb19d79e710c68eb02afe71978b7592947370"><titleInfo lang="eng"><title>Determination of trace elements in a human serum reference material by inductively coupled plasma mass spectrometry</title></titleInfo><name type="personal"><namePart type="given">Hans</namePart><namePart type="family">Vanhoe</namePart><affiliation>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent, Belgium</affiliation></name><name type="personal"><namePart type="given">Carlo</namePart><namePart type="family">Vandecasteele</namePart><role><roleTerm type="text">Research Director of the National Fund for Scientific Research (Belgium)</roleTerm></role><affiliation>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent, Belgium</affiliation></name><name type="personal"><namePart type="given">Jacques</namePart><namePart type="family">Versieck</namePart><affiliation>Department of Internal Medicine, Division of Gastroenterology, University Hospital, De Pintelaan 185, B-9000, Gent, Belgium</affiliation></name><name type="personal"><namePart type="given">Richard</namePart><namePart type="family">Dams</namePart><affiliation>Laboratory of Analytical Chemistry, Rijksuniversiteit Gent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000, Gent, Belgium</affiliation></name><typeOfResource>text</typeOfResource><genre>Original Papers</genre><genre>Original Paper</genre><originInfo><publisher>Springer-Verlag, Vienna</publisher><dateCreated encoding="w3cdtf">1989-02-16</dateCreated><dateValid encoding="w3cdtf">2005-02-16</dateValid><copyrightDate encoding="w3cdtf">1990</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="eng">A method was developed for the determination of Fe, Co, Cu, Zn, Rb, Mo and Cs in human serum by ICP-MS. Sample preparation was kept as limited as possible: Serum samples were diluted with nitric acid and indium was added as internal standard. The results for Fe, Co, Cu, and Zn were corrected for interferences from polyatomic ions using a suitable blank solution. No interferences occur for the considered isotopes of Rb, Mo, and Cs. A “second-generation human serum reference material” was analyzed, in order to test the accuracy and precision of the analytical procedure. The results obtained are in good agreement with the certified values.</abstract><subject lang="eng"><genre>Key words</genre><topic>ICP-MS</topic><topic>human serum</topic><topic>trace elements</topic><topic>accuracy</topic><topic>interferences</topic></subject><relatedItem type="series"><titleInfo type="abbreviated"><title>Mikrochim Acta</title></titleInfo><titleInfo><title>Microchimica Acta</title><subTitle>Micro and Trance Analysis</subTitle><partNumber>Year: 1990</partNumber><partNumber>Volume: 99</partNumber><partNumber>Number: 3-6</partNumber></titleInfo><genre>Archive Journal</genre><originInfo><dateIssued encoding="w3cdtf">1989-05-01</dateIssued><copyrightDate encoding="w3cdtf">1989</copyrightDate></originInfo><subject usage="primary"><topic>Chemistry</topic><topic>Analytical Chemistry</topic><topic>Inorganic Chemistry</topic><topic>Physical Chemistry</topic><topic>Characterization and Evaluation Materials</topic><topic>Monitoring/Environmental Analysis/Environmental Ecotoxicology</topic></subject><identifier type="issn">0026-3672</identifier><identifier type="issn">Electronic: 1436-5073</identifier><identifier type="matrixNumber">604</identifier><identifier type="local">IssueArticleCount: 31</identifier><recordInfo><recordOrigin>Springer-Verlag, 1989</recordOrigin></recordInfo></relatedItem><identifier type="doi">10.1007/BF01244693</identifier><identifier type="matrixNumber">Art24</identifier><identifier type="local">BF01244693</identifier><accessCondition type="use and reproduction">MetadataGrant: OpenAccess</accessCondition><accessCondition type="use and reproduction">AbstractGrant: OpenAccess</accessCondition><accessCondition type="restriction on access">BodyPDFGrant: Restricted</accessCondition><accessCondition type="restriction on access">BodyHTMLGrant: Restricted</accessCondition><accessCondition type="restriction on access">BibliographyGrant: Restricted</accessCondition><accessCondition type="restriction on access">ESMGrant: Restricted</accessCondition><part><extent unit="pages"><start>373</start><end>379</end></extent></part><recordInfo><recordOrigin>Springer-Verlag, 1990</recordOrigin><recordIdentifier>604_1990_Article_BF01244693.pdf</recordIdentifier></recordInfo></mods></record>Pour manipuler ce document sous Unix (Dilib)
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